Instrument is equipped with a Cu sealed tube and LYNXEYE XE-T detector.
These include a standard flat sample reflection holder, a 9-sample changer, a capillary holder, and a high temperature oven (100 C - 1200 C). Equipment for Powder Work:Ī high resolution versatile instrument which has several different sample holders. Instrument is equipped with a Moly rotating anode source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K. Instrument is equipped with a Gallium MetalJet source and a Photon III detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-500 K. Coming Soon.īruker D8 Venture Diffractometer-Ga MetalJet
#Bruker apex ii ccd detector generator
It is equipped with a Copper MicroMax 003f X-ray generator and PILATUS R200K Hybrid Pixel Array Detector as well as an Oxford Cryosystems Cobra for variable temperature data collection from 90-400 K. Instrument is currently located on the BioSide of campus. It has also facilitated the mutation of seeds, the examination of the radiation degradation effects of various compounds, and the performance of radiation damage studies in electronic components.Instrument is equipped with a Moly sealed tube and an Apex-II CCD detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-400 K.ĭual source instrument equipped with a TRIUMPH monochromated Moly sealed tube and a Copper IµS. System features a Kappa goniometer and a Photon II detector as well as an Oxford Cryosystems Cryostream for variable temperature data collection from 90-400 K.
The crystal-to-detector distance was 40.00 mm. The data were collected at 173 ☌, in 0.5° oscillations with 10 s exposures. Two separate gamma irradiation facilities located at the Center can be used for a wide array of research including cell, plasma, and biological material sterilization. All measurements were performed on a Bruker APEX-II CCD diractometer with a Cu K IS source. The data are compared to this model and the measured atomic structure so that bond lengths, bond angles, and atomic interactions can be modeled with great precision and accuracy. The X-rays, diffracting according to Bragg’s Law, are measured in terms of their intensity and exact origin on a CCD camera, and then are fitted to a computer model of the atomic crystal structure. Single crystal X-ray diffraction (SCXRD) uses X-ray radiation diffracting off of the electron clouds of atoms to determine the three-dimensional structure of a molecule or molecules in the solid-state. Solid-State Structural CharacterizationĪ Bruker Smart Apex II SCXRD system with an Apex2s CCD detector and an Oxford Cryosystems Cryostream 700 Controller is located onsite. Qualified staff members and researchers are available to aid in the best use of these specialized detectors. We maintain several alpha-particle spectrometers that can be used to determine quantities of the various isotopes of uranium, plutonium, americium, and thorium in most biological materials. The Center has many liquid nitrogen cooled high-purity germanium detectors that can run simultaneously for a host of NAA and gamma analysis needs.
It is especially useful for determining amounts of heavy metals – up to parts per billion – in samples often on the milligram scale. The diffraction data were collected at 100(2) K on a Bruker D8 three-circle diffractometer equipped with a SMART APEX II CCD detector and an INCOATEC Mo microsource with INCOATEC Quazar mirror. Neutron activation analysis (NAA) is a non-destructive gamma analysis method used to determine elemental concentrations in unknown samples.
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